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Development of vitamin K analysis method using column switching high-performance liquid chromatography method and analysis results of various food items for vitamin K content
http://hdl.handle.net/10458/0002000692
http://hdl.handle.net/10458/00020006927ead58f1-61d7-4cc0-b426-7f84b34cc7e2
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
article (1 MB)
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| Item type | 学術雑誌論文 / Journal Article(1) | |||||||
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| 公開日 | 2024-06-25 | |||||||
| タイトル | ||||||||
| タイトル | Development of vitamin K analysis method using column switching high-performance liquid chromatography method and analysis results of various food items for vitamin K content | |||||||
| 言語 | en | |||||||
| 言語 | ||||||||
| 言語 | eng | |||||||
| キーワード | ||||||||
| 言語 | en | |||||||
| 主題Scheme | Other | |||||||
| キーワード | Phylloquinone | |||||||
| キーワード | ||||||||
| 言語 | en | |||||||
| 主題Scheme | Other | |||||||
| キーワード | Menaquinone-4 | |||||||
| キーワード | ||||||||
| 言語 | en | |||||||
| 主題Scheme | Other | |||||||
| キーワード | Menaquinone-7 | |||||||
| キーワード | ||||||||
| 言語 | en | |||||||
| 主題Scheme | Other | |||||||
| キーワード | Column-switching HPLC | |||||||
| キーワード | ||||||||
| 言語 | en | |||||||
| 主題Scheme | Other | |||||||
| キーワード | Foods | |||||||
| キーワード | ||||||||
| 言語 | en | |||||||
| 主題Scheme | Other | |||||||
| キーワード | Supplements | |||||||
| 資源タイプ | ||||||||
| 資源タイプ | journal article | |||||||
| アクセス権 | ||||||||
| 著者 |
Tanaka, Rina
× Tanaka, Rina
× 田中, 竜介 |
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| 抄録 | ||||||||
| 内容記述タイプ | Abstract | |||||||
| 内容記述 | In this study, we developed a column-switching high-performance liquid chromatography (HPLC) method with fluorescence detection for the analysis of vitamin K. Column-switching is accomplished by changing the direction of flow using a switching valve with a set time program. Using this method, three vitamin K, phylloquinone (PK), menaquinone-4 (MK-4), and menaquinone-7 (MK-7), were separated and identified with high sensitivity, and impurities were eliminated. This method was used to determine the vitamin K content in meat, fish meat, snails, bivalves, sea urchins, seaweeds, vegetables, tea, soy products, milk products, and supplements. The results showed that chicken showed the highest content of MK-4 (15.35 ± 0.35 μg/100 g), matcha showed the highest content of PK (3069.66±80.10 μg/100 g), and dried natto showed the highest content of MK-7 (3997.57±79.42 μg/100 g). This method can also be used to analyze vitamin K in supplements and pharmaceuticals. The results of this study revealed that different manufacturers add different types of vitamin K to their commercial supplements and infant formulas. The developed method provides highly reproducible and quantitative results and allows for the rapid analysis of the three vitamin K types. Thus, the method developed in this study may aid the sequential analysis of vitamin K in different samples to assess food nutrients. | |||||||
| 言語 | en | |||||||
| 内容記述 | ||||||||
| 内容記述タイプ | Other | |||||||
| 内容記述 | Citation:Tanaka, R., Tanaka, R. Development of vitamin K analysis method using column switching high-performance liquid chromatography method and analysis results of various food items for vitamin K content. Food Anal. Methods (2024). https://doi.org/10.1007/s12161-024-02643-4 | |||||||
| 言語 | en | |||||||
| 書誌情報 |
en : Food Analytical Methods 巻 17, p. 1218-1228, 発行日 2024-06-11 |
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| 出版者 | ||||||||
| 出版者 | Springer Science and Business Media LLC | |||||||
| 言語 | en | |||||||
| ISSN | ||||||||
| 収録物識別子タイプ | ISSN | |||||||
| 収録物識別子 | 1936-9751 | |||||||
| ISSN | ||||||||
| 収録物識別子タイプ | EISSN | |||||||
| 収録物識別子 | 1936-976X | |||||||
| DOI | ||||||||
| 関連タイプ | isVersionOf | |||||||
| 識別子タイプ | DOI | |||||||
| 関連識別子 | https://doi.org/10.1007/s12161-024-02643-4 | |||||||
| 権利 | ||||||||
| 言語 | en | |||||||
| 権利情報 | © The Author(s) 2024 | |||||||
| 著者版フラグ | ||||||||
| 出版タイプ | VoR | |||||||
